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Physics Journal of the Indonesian Physical Society
http://situs.jurnal.lipi.go.id/pjhfi/   -   http://pj.hfi.fisika.net

STRUCTURE ANALYSIS OF CITATAH'S NATURAL CALCITE USING REITVELD METHOD

Y. Sudiana1, Irzaman2, H. Darmasetiawan2, S. Nurhasanah3, A. Arslan4.

1Akademi Kimia Analisis, Jl. Ir. H. Juanda 7, Bogor 16122, Indonesia
2Department of Physics, FMIPA IPB, Jl. Raya Pajajaran, Bogor-16144, Indonesia
3Department of Physics IPB Alumni
4Research and Development Centre for Material science and Technology, Nuclear Energy Agency (BATAN), Kawasan Puspiptek Serpong Tangerang, Banten, Indonesia

Abstract
Analytical data XRD has been carried out in the room temperature with refinement parameter Rietveld method on Citatah's natural calcite (CaCO3). We refined 25 parameters, which are scale factor (1), background parameters (6), zero point displacement (1), peak shape parameters U,V,W (3), FWHM coefficient (3), atomic position (9) and site occupancy (2). We obtained RBragg = 7.88 %. Experimental result shows that the crystalline structure was hexagonal with lattice parameter a = b = 4.9891 , c = 17.0424 , a = b = 90o and g = 120o and space group: R3c. The function of FWHM (H) = (0.82194 tan2q - 0.5416 tan q + 0.14375).

Publication : Physics Journal IPS Proceeding Supplement A6 (2002) 0539 » page of Content
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